Microflow photochemistry—a reactor comparison study using the photochemical synthesis of terebic acid as a model reaction
Shin, Aida, Terao, Kimitada, Nishiyama, Yasuhiro, Kakiuchi, Kiyomi, and Oelgemoeller, Michael (2012) Microflow photochemistry—a reactor comparison study using the photochemical synthesis of terebic acid as a model reaction. Tetrahedron Letters, 53 (42). pp. 5578-5581.
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DOI: 10.1016/j.tetlet.2012.07.143
View at Publisher Website: http://dx.doi.org/10.1016/j.tetlet.2012....
Abstract
The continuous-microflow photochemical synthesis of terebic acid from maleic acid was investigated in two different microreactor set-ups. The results were subsequently compared to analogue experiments in a conventional chamber reactor. Based on conversion rates, reactor design and energy efficiency calculations, the simple microcapillary reactor showed the best overall performance.
| ID Code: | 23374 |
|---|---|
| Item Type: | Article (Refereed Research - C1) |
| FoR Codes: | 03 CHEMICAL SCIENCES > 0305 Organic Chemistry > 030503 Organic Chemical Synthesis @ 25% 03 CHEMICAL SCIENCES > 0305 Organic Chemistry > 030505 Physical Organic Chemistry @ 25% 03 CHEMICAL SCIENCES > 0305 Organic Chemistry > 030504 Organic Green Chemistry @ 50% |
| SEO Codes: | 97 EXPANDING KNOWLEDGE > 970103 Expanding Knowledge in the Chemical Sciences @ 100% |
| Deposited On: | 14 Sep 2012 14:15 |
| Last Modified: | 30 Apr 2013 02:13 |
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| Citation Counts with External Providers: | Web of Science: 1 |
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